Webb2.2. Synthesis of the hierarchical ZSM-5 zeolites In the typical synthesis method of hierarchical ZSM-5 zeolites, the mesoporogen OPA was added to the solution of 22.11 g silica sol (40 wt% SiO 2, Guangdong Huihe Silicon Products Co., Ltd) (or 30.7 g tetraethylorthosilicate (TEOS), Shanghai Silicon Mountain Macromolecular Materials … Webb1 dec. 2024 · The H-form ZSM-5 zeolites were directly obtained after filtration, drying, and heating at 550 °C for 4 h without performing the ion-exchange and calcination steps. …
Direct synthesis of [B,H]ZSM-5 by a solid-phase method: Al
Webb8 apr. 2010 · Phosphorus (P) modified H-ZSM-5 catalysts were prepared by wet impregnation method by varying P loadings from 0 to 7.43 wt % using phosphoric acid … Webb24 feb. 2024 · In this paper, Ce and Zr modified commercial SAPO-34 and H-ZSM-5 catalysts were synthesized via a wet impregnation method and used as catalysts for the production of light olefins from naphtha. The synthesized catalysts were characterized using SEM, TGA, XRD, BET, and NH 3 -TPD. Thermal catalytic cracking of parent … shoosh com
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Webb7 dec. 2024 · The traditional hydrothermal synthesis strategy of ZSM-5 zeolite is energy-consumption accompanying by pollution issues. Herein, phosphorus-modified layered ZSM-5 zeolites (PZ) were obtained by one-pot synthesis under solvent-free conditions. The synthesized samples were fully characterized by XRD, SEM, BET, NH3-TPD and … Webb1 mars 2024 · I am currently working as an Assistant Professor in the chemical engineering department at the Quaid-e-Awam University of … High silica H-ZSM-5 catalysts were synthesized by the hydrothermal method using silicic acid and sodium aluminate as Si and Al sources, respectively. The molar ratio of the starting gel was 20SiO 2 :0.05Al 2 O 3 :xTPAOH:yTPABr:1.5Na 2 O:200H 2 O, where x + y = 1.0. Visa mer Thermo-gravimetric/differential thermal analysis (TGA/DTA) were performed aiming to examine the complete elimination of organic … Visa mer Nitrogen adsorption–desorption isotherm measurements were carried out at 77 K in order to investigate the effect of template composition on the textural properties of ZSM-5. Fig. 3 illustrates the N2 adsorption–desorption … Visa mer Fig. 1 displays the X-ray diffraction patterns of the H-ZSM-5 catalysts. All samples showed XRD patterns that are typical of the MFI-structure for H-ZSM-5. It must be noted that almost all the samples had some impurity. … Visa mer The FT-IR spectra of the H-ZSM-5 catalysts with different combinations of the two templates were recorded in the range of 400–4000 cm−1. Using the FT-IR bands, useful information can be achieved on the framework … Visa mer shoosh clipart